Ester value

From WaxPedia
Revision as of 13:15, 9 April 2013 by Wikimc (Talk | contribs)

Jump to: navigation, search

The ester value is the number of mg of potassium hydroxide required to saponify the esters in 1.0 g of the substance.[1]


Wax esters

Wax esters are oxoesters of long-chain fatty acids esterified with long-chain alcohols. The ester value shows the amount alkali consumed in the saponification of the esters[2] and is possible identify and differentiate the waxes with this value; for example beeswax ester value is 72 to 79 mg KOH/ g, candelilla wax ester value is 31 to 43 mg KOH/g and carnauba wax ester value is 74 to 78 mg KOH/g.


Method

In ester value determination, the sample is hydrolysed to alcohol and using excess of standar potassium hydroxide solution. The excess of alkali is back titrated. USP-NF monographs presents a general procedure of ester value apply to fats, fixed oils and waxes.


USP 401

.[1]


Referencia

  1. 1.0 1.1 Warth, A. H.; The Chemistry and Technology of Waxes. Reinhold Publishing Corporation. Second Edition, p.586
  2. Pharmacopedia/National Formulary. US., Vol. 1, 2009, p. 150